Lab Equipment
Centrifuges
Diameter: 5 inches
Description: Kynar-coated Steel
Diameter: 5 inches
Description: Stainless Steel
Reactors
Type: 72 Liter Glass
Description: Reaction vessel & 4” dia packed fractionation column with reflux splitter; full vacuum and heating mantle.
Type: 27 Liter Glass
Description: Resin flask with multiple port head; full vacuum and heating mantle; overhead stirrer.
Type: 22 Liter Glass
Description: Reaction vessel & 3” dia packed fractionation column with reflux splitter; full vacuum and heating mantle.
Type: 22 Liter Glass
Description: Several vessels with one to three necks for multi-purpose operations; full vacuum.
Type: 12 Liter Glass
Description: Several vessels with one to three necks for multi-purpose operations; full vacuum.
Type: Bantamware
Description: Extensive microbore glassware from 2 to 100mL with multiple necks; full vacuum; molecular still.
Type: Smaller Glass
Description: 5 Liter down to microbore sizes with multiple necks; full vacuum.
Type: 2 L Hastelloy
Description: Autoclave to 2000 psi or full vacuum; thermostat-controlled external heating and/or internal heating/cooling coil; magnetically-driven agitation.
Type: 2 L Stainless Steel
Description: Autoclave to 2000 psi or full vacuum; thermostat-controlled external heating and/or internal heating/cooling coil; magnetically-driven agitation.
Type: 500 mL
Description: Parr Shaker Apparatus; glass to 60 psi.
Distillation
Type: Columns
Description: Several to 48” with various diameters; 1- 1.5” dia x 48”, vacuum-jacketed & silvered with spherical joints.
Type: Heads
Description: Four with magnetic, adjustable reflux splitters & T/S 29/42 joints & condensers.
Ovens
Type: Atmospheric
Description: Horizontal air flow; to 200°C; Stainless Steels.
Size: 5 sq. ft.
Type: Atmospheric
Description: Gravity convection; to 250°C; Stainless Steel.
Size: 1 sq. ft.
Type: Atmospheric
Description: Lab-line incubator; 30°C to 65°C; Stainless Steel.
Size: 1 sq. ft.
Type: Vacuum
Description: To 250°C; Stainless Steel.
Size: 2 sq. ft.
Type: Vacuum
Description: To 60°C; Stainless Steel Dryer.
Size: 12 sq. ft.
Type: Vacuum
Description: To 200°C.
Size: 1 sq. ft.
Vacuum Pumps
Brand: Kinney
Description: Auxiliary unit for kilo lab; high capacity.
Brand: Kinney
Description: Integrated with 72 L reaction unit; high capacity.
Brand: Ingersol Rand
Description: Laboratory house vac system; high capacity.
Brand: Precison
Description: Model DD 90; 3.2 CFM
Brand: Precison
Description: Model D 150; 5.3 CFM
Brand: Duo Seal (Welch)
Description: Model 1397; SN 6153-97; high capacity
QC & Non-QC Instrumentation & Apparatus
Refractometer: Reichert AR200 Digital
Orion Ion Specific Electrodes (K, Na, Ag and halides)
Balances:
Mettler XPE-105
Mettler AG-135
Mettler MS 6001S (top-loading digital LCD) (2)
Mettler PC 24 (top-loading digital LCD)
Mettler ICS425 (top-loading digital LCD)
Karl-Fischer Apparatus:
Mettler Toledo V205 Karl-Fischer Titrator
Melting Point Apparatus:
Bibby Electrothermal
Mel-Temp
Purge and Trap:
Tekmar Velocity XPT
Gas Chromatographs:
Bruker 450 GC S/S & universal (on column) injectors (1)
Scion 456 S/S & universal (on column) injectors (2)
Combi-Pal Auto injector (2)
GCMS:
Finnegan TRACE CCMS with Edwards RV3 roughing pump
HPLC:
Hewlett-Packard 1100 (variable UV & Refractive Index detectors)
Agilent 1200 (variable UV detector)
pH Meters:
Orion 320 (2)
Conductivity Meter:
Oakton Con 150
Spectrophotometers:
Brusker Alpha FTIR
P-E UV/Vis Lambda 25
Muffle Furnace:
Thermolyne 83000
Software/Data Systems:
Several individual PCs are linked to the instrumentation to control operations, collect, store and retrieve data, and facilitate methods development. The GC Compass software and HPLC Agilent software ensure GMP compliance.